吴海辰, 陈国新, 于海涛, 沈圣成, 梁芮, 卢焕明. 纯锌中变形孪晶界精细结构的透射电子显微镜表征[J]. 分析测试技术与仪器, 2022, 28(3): 247-253. DOI: 10.16495/j.1006-3757.2022.03.003
引用本文: 吴海辰, 陈国新, 于海涛, 沈圣成, 梁芮, 卢焕明. 纯锌中变形孪晶界精细结构的透射电子显微镜表征[J]. 分析测试技术与仪器, 2022, 28(3): 247-253. DOI: 10.16495/j.1006-3757.2022.03.003
WU Hai-chen, CHEN Guo-xin, YU Hai-tao, SHEN Sheng-cheng, LIANG Rui, LU Huan-ming. Characterization of Microstructure of Deformation Twin Boundary in Zinc by Transmission Electron Microscopy[J]. Analysis and Testing Technology and Instruments, 2022, 28(3): 247-253. DOI: 10.16495/j.1006-3757.2022.03.003
Citation: WU Hai-chen, CHEN Guo-xin, YU Hai-tao, SHEN Sheng-cheng, LIANG Rui, LU Huan-ming. Characterization of Microstructure of Deformation Twin Boundary in Zinc by Transmission Electron Microscopy[J]. Analysis and Testing Technology and Instruments, 2022, 28(3): 247-253. DOI: 10.16495/j.1006-3757.2022.03.003

纯锌中变形孪晶界精细结构的透射电子显微镜表征

Characterization of Microstructure of Deformation Twin Boundary in Zinc by Transmission Electron Microscopy

  • 摘要: 运用透射电子显微镜对密排六方的纯锌中由变形引发的10 \overline1 2 孪晶界精细结构进行了表征,发现实际孪晶界会在宏观尺度上大幅偏离理论孪晶面. 高分辨透射电子显微镜分析表明,实际孪晶界可以由(10 \overline1 2 )共格孪晶面和小段基面/柱面(BP/PB)台阶相互连接组成,也可以仅由一系列相互垂直的BP/PB台阶连接而成. 这两种结构不同的孪晶界可以共存于同一个10 \overline1 2 孪晶中. 结合位错理论对两种孪晶界的迁移机制进行了讨论,第一种孪晶界的迁移是通过孪生位错在共格孪晶界上运动和界面位错在BP/PB台阶上运动来实现的,第二种孪晶界则要通过局部晶胞重构机制实现迁移. 两种孪晶界的共存可以由孪晶的形核和生长过程解释.

     

    Abstract: The microstructure of 10\bar 12 twin boundary in zinc induced by severe plastic deformation was characterized using transmission electron microscope (TEM). The result showed that the actual twin boundary can deviate significantly from the theoretical twinning plane. By high resolution TEM analysis, the actual twin boundaries consist of (10\bar 12 ) coherent twin boundary (CTB) connected with short BP/PB facets, or only consist of a series of BP/PB facets perpendicular to each other. These two kinds of twin boundaries with different microstructures can coexist stably in a 10\bar 12 twin. Based on the dislocation theory, the migration mechanism of these two kinds of twin boundaries was discussed. For the first kind of twin boundary, the migration can be accomplished via the motion of twinning dislocation on the CTB together with the motion of interface dislocation on the BP/PB facets. For the second kind of twin boundary, the migration is accomplished via a unit cell reconstruction mechanism. The coexistence of the two kinds of twin boundaries can be explained based on the nucleation and growth process of a 10\bar 12 twin.

     

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