WeChat
Volume 28 Issue 2
Jun.  2022
Turn off MathJax
Article Contents
KEN Sheng-ye, DUAN Qin, SU Dan-dan, YANG Yi, TIAN Fei-yu, YANG Xue-yan. Determination of Nicotine in Tobacco Concrete by Gas Chromatography[J]. Analysis and Testing Technology and Instruments, 2022, 28(2): 205-209. doi: 10.16495/j.1006-3757.2022.02.015
Citation: KEN Sheng-ye, DUAN Qin, SU Dan-dan, YANG Yi, TIAN Fei-yu, YANG Xue-yan. Determination of Nicotine in Tobacco Concrete by Gas Chromatography[J]. Analysis and Testing Technology and Instruments, 2022, 28(2): 205-209. doi: 10.16495/j.1006-3757.2022.02.015

Determination of Nicotine in Tobacco Concrete by Gas Chromatography

doi: 10.16495/j.1006-3757.2022.02.015
  • Received Date: 2022-03-08
  • Rev Recd Date: 2022-05-12
  • Available Online: 2022-07-07
  • Publish Date: 2022-06-30
  • A gas chromatography-flame ionization (GC-FID) method has been developed for the determination of nicotine in the tobacco concrete using 2-methylquinoline as the internal standards, five tobacco concrete samples were determined. The results showed that the limit of detection and limit of quantitation were 0.27 mg/g and 0.89 mg/g, respectively. The recoveries were 95.00%~98.58%. The contents of nicotine in the samples ranged from 19.66~54.97 mg/g. The method is easy, sensitive and accurate, and is suitable for the determination of nicotine in the tobacco concrete.
  • loading
  • [1]
    朱苏闽, 李军, 林平. 固相微萃取-气相色谱-质谱法分析云烟浸膏和烟末浸膏的挥发性化学成分[J]. 质谱学报, 2004, 25(1): 32-37. doi: 10.3969/j.issn.1004-2997.2004.01.007

    ZHU Su-min, LI Jun, LIN Ping. Identification of volatile components in Yunyan and yanmo concrete by solid-phase microextraction-gas chromatography-mass spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2004, 25(1): 32-37. doi: 10.3969/j.issn.1004-2997.2004.01.007
    [2]
    谢剑平. 烟草与烟气化学成分[M]. 北京: 化学工业出版社, 2011.
    [3]
    廖坤, 彭春鸣, 张翼, 胡炜. 气相色谱法测定烟草中的烟碱含量[J]. 烟草科技, 2003, 36(3): 32-34. doi: 10.3969/j.issn.1002-0861.2003.03.011

    LIAO Kun, PENG Chun-ming, ZHANG Yi, HU Wei. Determination of nicotine in tobacco with gas chromatography[J]. Tobacco Science & Technology, 2003, 36(3): 32-34. doi: 10.3969/j.issn.1002-0861.2003.03.011
    [4]
    罗琼, 李青. 高效液相色谱法测定烟草中烟碱含量[J]. 现代农业科技, 2018(8): 242, 246. https://www.cnki.com.cn/Article/CJFDTOTAL-ANHE201808152.htm

    LUO Qiong, LI Qing. Determination of nicotine content in tobacco by high performance liquid chromatography[J]. Modern Agricultural Science and Technology, 2018(8): 242, 246. https://www.cnki.com.cn/Article/CJFDTOTAL-ANHE201808152.htm
    [5]
    赵立红, 方敦煌. 连续流动分析法测定烟草中水溶性糖、烟碱、氯离子的比较研究[J]. 光谱实验室, 2007, 24(2): 224-230. doi: 10.3969/j.issn.1004-8138.2007.02.050

    ZHAO Li-hong, FANG Dun-huang. Study on water-soluble sugars, nicotine and chlorion in tobacco by different continuous flow analyzers[J]. Chinese Journal of Spectroscopy Laboratory, 2007, 24(2): 224-230. doi: 10.3969/j.issn.1004-8138.2007.02.050
    [6]
    王家俊. FT-NIR光谱分析技术测定烟草中总氮、总糖和烟碱[J]. 光谱实验室, 2003, 20(2): 181-185. doi: 10.3969/j.issn.1004-8138.2003.02.004

    WANG Jia-jun. Determination of total-nitrogen, total-sugar and nicotine in tobacco by FT-NIR spectrometry[J]. Chinese Journal of Spectroscopy Laboratory, 2003, 20(2): 181-185. doi: 10.3969/j.issn.1004-8138.2003.02.004
    [7]
    蔡君兰, 陈黎, 彭斌, 余晶晶, 崔华鹏, 王冰, 张晓兵, 刘惠民, 刘绍锋. 气相色谱法同时测定电子烟烟液中的烟碱、1, 2-丙二醇和丙三醇[J]. 中国烟草学报, 2016, 22(5): 1-9. https://www.cnki.com.cn/Article/CJFDTOTAL-ZGYB201605002.htm

    CAI Jun-lan, CHEN Li, PENG Bin, YU Jing-jing, CUI Hua-peng, WANG Bing, ZHANG Xiao-bing, LIU Hui-min, LIU Shao-feng. Simultaneous determination of nicotine, 1, 2- propylene glycol and glycerol in e-liquids with gas chromatography method[J]. ActaTabacariaSinica, 2016, 22(5): 1-9. https://www.cnki.com.cn/Article/CJFDTOTAL-ZGYB201605002.htm
    [8]
    段沅杏, 赵伟, 杨威, 洪鎏, 田永峰, 杨继, 陈永宽, 杨柳. 口用型无烟气烟草制品中烟碱的测定[J]. 烟草科技, 2017, 50(7): 69-75. https://www.cnki.com.cn/Article/CJFDTOTAL-YCKJ201707010.htm

    DUAN Yuan-xing, ZHAO Wei, YANG Wei, HONG Liu, TIAN Yong-feng, YANG Ji, CHEN Yong-kuan, YANG Liu. Determination of nicotine in oral smokeless tobacco products[J]. Tobacco Science & Technology, 2017, 50(7): 69-75. https://www.cnki.com.cn/Article/CJFDTOTAL-YCKJ201707010.htm
    [9]
    赵光飞, 刘静, 屠彦刚, 陈华, 任俞澄, 吴建霖, 陈绍全, 陈宇超, 李锐, 张一扬, 周桂园. 气相色谱法同时检测加热不燃烧卷烟芯材中的1, 2-丙二醇、烟碱与甘油含量[J]. 中国测试, 2019, 45(3): 69-74. https://www.cnki.com.cn/Article/CJFDTOTAL-SYCS201903013.htm

    ZHAO Guang-fei, LIU Jing, TU Yan-gang, CHEN Hua, REN Yu-cheng, WU Jian-lin, CHEN Shao-quan, CHEN Yu-chao, LI Rui, ZHANG Yi-yang, ZHOU Gui-yuan. Simultaneous determination of 1, 2-propylene glycol, nicotine and glycerol in heat-not-burn cigarette core material by gas chromatography method[J]. China Measurement & Test, 2019, 45(3): 69-74. https://www.cnki.com.cn/Article/CJFDTOTAL-SYCS201903013.htm
    [10]
    温光和, 肯生叶, 李峰, 饶国华, 段勤, 杨雪燕, 田飞宇. 加热不燃烧卷烟烟草材料中1, 2-丙二醇、丙三醇和烟碱的测定[J]. 中国烟草科学, 2019, 40(4): 69-75. https://www.cnki.com.cn/Article/CJFDTOTAL-ZGYV201904012.htm

    WEN Guang-he, KEN Sheng-ye, LI Feng, RAO Guo-hua, DUAN Qin, YANG Xue-yan, TIAN Fei-yu. Determination of 1, 2-propylene glycol, glycerol and nicotine of tobacco materials in heat-not-burn cigarettes[J]. Chinese Tobacco Science, 2019, 40(4): 69-75. https://www.cnki.com.cn/Article/CJFDTOTAL-ZGYV201904012.htm
    [11]
    国家质量监督检验检疫总局, 中国国家标准化管理委员会. 合格评定化学分析方法确认和验证指南: GB/T 27417—2017[S]. 北京: 中国标准出版社, 2017.

    General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China. Comformity assessment—Guidance on validation and verification of chemical analytical methods: GB/T 27417—2017[S]. Beijing: Standards Press of China, 2017.
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(6)  / Tables(3)

    Article Metrics

    Article views (44) PDF downloads(9) Cited by()
    Proportional views
    Related

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return