WANG Hai-rui, CHEN Shao-bo, XU Zhen-dong. Simultaneous Determination of 10 Dye Components in Hair Dye by High Performance Liquid Chromatography[J]. Analysis and Testing Technology and Instruments, 2018, 24(1): 28-33. DOI: 10.16495/j.1006-3757.2018.01.005
Citation: WANG Hai-rui, CHEN Shao-bo, XU Zhen-dong. Simultaneous Determination of 10 Dye Components in Hair Dye by High Performance Liquid Chromatography[J]. Analysis and Testing Technology and Instruments, 2018, 24(1): 28-33. DOI: 10.16495/j.1006-3757.2018.01.005

Simultaneous Determination of 10 Dye Components in Hair Dye by High Performance Liquid Chromatography

  • In this article a simultaneous analytical method for the detection of P-phenylene diamine and other 10 oxidation type dye components in hair dye by high performance liquid chromatography is described. The objectives of dye derivatives p-phenylenediamine, resorcine, p-aminopheno, m-aminophenol, 4-amino-m-cresol, hydroquinone, 4-amino-2-hydroxytoluene, p-diamino-2-nitrobenzene, 2, 5-diaminotoluene sulfate, 6-hydroxyindole were seperated on a Poroshell 120 Bonus-RP capillary column. Mass spectrometry was used to quantify the dye in hair dye. Results showed that correlation coefficients of the method were from 0.999 85 to 0.999 96. The relative standard deviation(RSD) was less than 5.91% when the concentrations were in the range of 0.01~0.5 mg/mL, the recovery was from 87.2% to 106.7%. The determination results demonstrated that the method had the feature of simple, rapid, and higly selective.
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