Simultaneous Determination of 10 Dye Components in Hair Dye by High Performance Liquid Chromatography

WANG Hai-rui; CHEN Shao-bo; XU Zhen-dong

doi:10.16495/j.1006-3757.2018.01.005

Issue 1

Turn off MathJax

Article Contents

Article Navigation > Analysis and Testing Technology and Instruments > 2018 > 24(1): 28-33

WANG Hai-rui, CHEN Shao-bo, XU Zhen-dong. Simultaneous Determination of 10 Dye Components in Hair Dye by High Performance Liquid Chromatography[J]. Analysis and Testing Technology and Instruments, 2018, 24(1): 28-33. doi: 10.16495/j.1006-3757.2018.01.005

Citation:

WANG Hai-rui, CHEN Shao-bo, XU Zhen-dong. Simultaneous Determination of 10 Dye Components in Hair Dye by High Performance Liquid Chromatography[J]. Analysis and Testing Technology and Instruments, 2018, 24(1): 28-33. doi: 10.16495/j.1006-3757.2018.01.005

Citation:

PDF( 1213 KB)

Simultaneous Determination of 10 Dye Components in Hair Dye by High Performance Liquid Chromatography

doi: 10.16495/j.1006-3757.2018.01.005

WANG Hai-rui^{1, 2
,},
CHEN Shao-bo^{1, 2},
XU Zhen-dong¹

1.
Comprehensive Technology Center of Suzhou Entry and Exit Inspection and Quarantine Bureau, Suzhou 215104 Jiangsu China
2.
Suzhou World Standard Testing Technology Co Ltd., Suzhou 215104, Jiangsu China

Received Date: 2017-12-05
Rev Recd Date: 2018-03-12
Publish Date: 2018-03-01

Abstract

Abstract

In this article a simultaneous analytical method for the detection of P-phenylene diamine and other 10 oxidation type dye components in hair dye by high performance liquid chromatography is described. The objectives of dye derivatives p-phenylenediamine, resorcine, p-aminopheno, m-aminophenol, 4-amino-m-cresol, hydroquinone, 4-amino-2-hydroxytoluene, p-diamino-2-nitrobenzene, 2, 5-diaminotoluene sulfate, 6-hydroxyindole were seperated on a Poroshell 120 Bonus-RP capillary column. Mass spectrometry was used to quantify the dye in hair dye. Results showed that correlation coefficients of the method were from 0.999 85 to 0.999 96. The relative standard deviation(RSD) was less than 5.91% when the concentrations were in the range of 0.01~0.5 mg/mL, the recovery was from 87.2% to 106.7%. The determination results demonstrated that the method had the feature of simple, rapid, and higly selective.
- hair dye,
- dye,
- high performance liquid chromatography

FullText(HTML)

References(11)

References

刘丽, 李英, 刘志红, 等.超声波抽提气相色谱-质谱法测定氧化型染发剂中16种染料[J].分析化学, 2004, 32(10):1333-1336. doi: 10.3321/j.issn:0253-3820.2004.10.016

LIU Li, LI Ying, LIU Zhi-hong, et al. Determination of colorants in oxidation hair dyes by gas chromatography-mass spectrometry[J]. Chinese Journal of Analytical Chemistry, 2004, 32(10):1333-1336. doi: 10.3321/j.issn:0253-3820.2004.10.016

李艳松, 徐静.气相色谱法测定染发剂中的对苯二胺[J].分析与检测, 2008, 90(6):92-93. https://www.wenkuxiazai.com/doc/3f963647be1e650e52ea999e.html

LI Yan-song, XU Jing. Determination of p-p henylenediamine in hair dyes by gas chromatography spectrometry[J]. Analysis and Detection, 2008, 90(6):92-93. https://www.wenkuxiazai.com/doc/3f963647be1e650e52ea999e.html

李海涛, 吴平谷.气相色谱法测定氧化型染发剂中染料[J].中国卫生检验杂志, 2002, 12(4):435. http://www.mat-test.com/abstract.htm?aid=OJ150105000377SoUrXu

LI Hai-tao, WU Ping-gu. Determination of dye in oxidation hair dyes by gas chromatography spectrometry[J]. Chinese Health Laboratory Technology, 2002, 12(4):435. http://www.mat-test.com/abstract.htm?aid=OJ150105000377SoUrXu

朱会卷, 杨艳伟, 张卫强, 等.高效液相色谱法测定染发剂中的22种染料成分[J].色谱, 2008, 26(5):554-558. http://www.mat-test.com/abstract.htm?aid=OJ150105000377SoUrXu

ZHU Hui-jiuan, YANG Yan-wei, ZHANG Wei-qiang, et al. Determination of 22 components in hair dyes by high performance liquid chromatography[J]. Chinese Jourmal of Chromatography, 2008, 26(5):554-558. http://www.mat-test.com/abstract.htm?aid=OJ150105000377SoUrXu

廖军海, 何孟杭, 欧阳立群, 等.高效液相色谱法同时测定染发剂中10种酸性染料[J].福建分析测试, 2015, 24(1):11-15. http://d.wanfangdata.com.cn/Periodical_fjfxcs201501004.aspx

LIAO Jun-hai, HE Meng-hang, OUYANG Li-qun, et al. Determination of ten acid dyes in hair dyes by high performance liquid chromatography[J]. Fujian Analysis & Testing, 2015, 24(1):11-15. http://d.wanfangdata.com.cn/Periodical_fjfxcs201501004.aspx

陈希, 张国文.高效液相色谱法测定染发剂中的12种有机胺类染料[J].南昌大学学报, 2014, 38(2):143. http://d.wanfangdata.com.cn/Periodical_ncdxxb201402010.aspx

CHEN Xi, ZHANG Guo-wen. Determination of 12 kinds of organic amine dyes in hair dyes by HPLC method[J]. Journal of Nanchang University, 2014, 38(2):143. http://d.wanfangdata.com.cn/Periodical_ncdxxb201402010.aspx

冯靓, 王立媛, 应英, 等.高效液相色谱法同时测定染发剂中13种染料[J].中国卫生检疫杂志, 2011, 21(6):1352-1354. http://www.cqvip.com/QK/98046X/201106/38358481.html

FENG Liang, WANG Li-yuan, YING Ying, et al. Simultaneous determination of 12 colorants in hair dyes by HPLC[J]. Chinese Journal of Health Laboratory Technology, 2011, 21(6):1352-1354. http://www.cqvip.com/QK/98046X/201106/38358481.html

朱英, 杨艳伟, 李静, 等.气相色谱-质谱法同时测定氧化型染发剂中多种染料中间体[J].色谱, 2005, 25(5):566. http://d.wanfangdata.com.cn/Periodical_gdxxhxxb201110011.aspx

ZHU Ying, YANG Yan-wei, LI Jing, et al. Simultaneous determination of variety dye intermediate in oxidation hair dyes by gas chromatography-mass spectrometry[J]. Chinese Jourmal of Chromatography, 2005, 25(5):566. http://d.wanfangdata.com.cn/Periodical_gdxxhxxb201110011.aspx

赖莺, 陈和秀, 林睿, 等.气相色谱-质谱法同时测定氧化型染发剂中的17种染料[J].高等学校化学学报, 2011, 32(10):2286-2292. http://d.wanfangdata.com.cn/Periodical_gdxxhxxb201110011.aspx

LAI Ying, CHEN He-xiu, LIN Rui, et al. Simultaneous determination of 17 components in oxidative hair dyes by gas chromatography-mass spectrometry[J].Chemical Journal of Chinese Universites, 2011, 32(10):2286-2292. http://d.wanfangdata.com.cn/Periodical_gdxxhxxb201110011.aspx

邵超英, 秦婷, 孙多志, 等.高效液相色谱-串联质谱法测定染发剂中11种苯胺和苯酚类染料[J].分析化学, 2014, 42(5):781-782. http://www.cnki.com.cn/Article/CJFDTotal-FXHX201405034.htm

SHAO Chao-ying, QIN Ting, SUN Duo-zhi, et al. Determination of 11 kinds of phenol and amine dyes in oxidative hair dyes by high performance liquid chromatography-tandem mass spectrometry[J]. Chinese Journal of Analytical Chemisty, 2014, 42(5):781-782. http://www.cnki.com.cn/Article/CJFDTotal-FXHX201405034.htm

陈梦, 胡磊, 许立, 等.高效液相色谱-质谱法同时测定染发剂中33种禁限用染料[J].日用化学工业, 2016, 46(6):359-364. http://www.chrom-china.com/CN/abstract/abstract13373.shtml

CHEN Meng, HU Lei, XU Li, et al. Simultaneous determination of 33 kinds of banned and/or restricted component in hair dyes by high performance liquid chromatography-mass spectrometry[J]. China Surfactant Delergent & Cosmetics, 2016, 46(6):359-364. http://www.chrom-china.com/CN/abstract/abstract13373.shtml

Relative Articles

Supplements(0)

Cited By

Proportional views