谭亮, 陈涛, 杲秀珍, 赵静, 贺明珠, 李玉林. 多通道可回收型中试亚临界流体萃取装置的改造及功能拓展[J]. 分析测试技术与仪器, 2019, 25(4): 219-227. DOI: 10.16495/j.1006-3757.2019.04.002
引用本文: 谭亮, 陈涛, 杲秀珍, 赵静, 贺明珠, 李玉林. 多通道可回收型中试亚临界流体萃取装置的改造及功能拓展[J]. 分析测试技术与仪器, 2019, 25(4): 219-227. DOI: 10.16495/j.1006-3757.2019.04.002
TAN Liang, CHEN Tao, GAO Xiu-zhen, ZHAO Jing, HE Ming-zhu, LI Yu-lin. Modification and Development of Multichannel Recyclable Pilot Sub-Critical Fluid Extraction Device[J]. Analysis and Testing Technology and Instruments, 2019, 25(4): 219-227. DOI: 10.16495/j.1006-3757.2019.04.002
Citation: TAN Liang, CHEN Tao, GAO Xiu-zhen, ZHAO Jing, HE Ming-zhu, LI Yu-lin. Modification and Development of Multichannel Recyclable Pilot Sub-Critical Fluid Extraction Device[J]. Analysis and Testing Technology and Instruments, 2019, 25(4): 219-227. DOI: 10.16495/j.1006-3757.2019.04.002

多通道可回收型中试亚临界流体萃取装置的改造及功能拓展

Modification and Development of Multichannel Recyclable Pilot Sub-Critical Fluid Extraction Device

  • 摘要: 以中试亚临界流体萃取装置为基础,将萃取金属滤筐改造为多通道非对称性微孔复合陶瓷膜滤芯、增加萃取溶剂回收系统以及相关重要部件的安装与调试,实现了系统压力在1.55±0.05 Mpa范围内波动,稳定可控.植物油萃取效率提高到95%以上,平均提取时间缩短了75%左右.对植物油中脂肪酸、挥发性有效成分可进行准确定性、定量分析.平均回收率在93%左右,实现了萃取溶剂有效回收利用,节能减排,从而实现了仪器的多通道可回收型升级改造,达到了仪器萃取能力提升的目的.

     

    Abstract: Based on the pilot sub-critical fluid extraction device, through the modification of metal filter basket for extraction to the multichannel asymmetric microporous composite ceramic membrane filter element, the increase of extraction solvent recovery system and the installation and adjustment of relevant important parts, the qualitative and quantitative analysis of fatty acids and volatile active components in plant oil can be realized accurately, and the system pressure was fluctuated within 1.55±0.05 Mpa and was stable and controllable, the extraction efficiency of plant oil was increased to more than 95%, the average extraction time was shortened by about 75%. The average recovery was about 93%, the effective recovery and utilization of extraction solvent, the energy conservation and emissions reduction can also be realized. Thus, the escalation and modification of the multichannel recyclable mode instrument is realized, and the purpose of increasing the extraction capacity of the instrument is achieved.

     

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