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祝建国,张涛,陈世焱,毛振才. 金矿石中高含量锑的断续流动氢化物发生-原子荧光光谱法快速测定[J]. 分析测试技术与仪器, 2009, 15(3).
引用本文: 祝建国,张涛,陈世焱,毛振才. 金矿石中高含量锑的断续流动氢化物发生-原子荧光光谱法快速测定[J]. 分析测试技术与仪器, 2009, 15(3).
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ZHU Jian-guo,ZHANG Tao,CHEN Shi-yan,MAO Zhen-cai. Rapid Determination of High Content Sb in Gold Ore with Interrupted Flow by Hydride Generation-Atomic Fluorescence Spectrometry[J]. Analysis and Testing Technology and Instruments, 2009, 15(3).
Citation: ZHU Jian-guo,ZHANG Tao,CHEN Shi-yan,MAO Zhen-cai. Rapid Determination of High Content Sb in Gold Ore with Interrupted Flow by Hydride Generation-Atomic Fluorescence Spectrometry[J]. Analysis and Testing Technology and Instruments, 2009, 15(3).
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金矿石中高含量锑的断续流动氢化物发生-原子荧光光谱法快速测定

Rapid Determination of High Content Sb in Gold Ore with Interrupted Flow by Hydride Generation-Atomic Fluorescence Spectrometry

    摘要
  • 摘要: 采用王水(1+1)水浴分解样品,氢化物发生一原子荧光光谱法(HG-AFS)测定金矿石中高含量的锑.其方法回收率在95.0%～102.0%之间,相对标准偏差在1.0%～3.4%之间,方法检出限为3.0×10-10g/mL,经试验证实该方法可测范围宽、简便、快速、准确,实验室间对比分析结果吻合程度令人满意.

     

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